PART Ⅰ INSTRUMENTAL ANALYSIS

CHAPTER 1 GENERALIZATION OF INSTRUMENTAL ANALYSIS

1.1 GENERALIZATION OF MODERN ANALYTICAL TECHNOLOGY

1.2 CHARACTERICS OF MODERN ANALYTICAL TECHNOLOGY

1.3 DEVELOPMENT OF MODERN ANALYTICAL TECHNOLOGY

CHAPTER 2 GAS CHROMATOGRAPHIC ANALYTICAL TECHNOLOGY

2.1 GENERALIZATION

2.2 BASIC PRINCIPLE OF GAS CHROMATOGRAPHY

2.3 DETERMINATION OF UDMH WITH GAS CHROMATOGRAPHY

CHAPTER 3 GAS CHROMATOGRPHY-MASS SPECTROSCOPY COMBINATION ANALYTICAL TECHNOLOGY

3.1 GENERALIZATION

3.2 BASIC PRINCIPLE OF GAS CHROMATOGRAPHY-MASS SPECTROSCOPY COMBINATION

3.3 DETERMINATION OF THE OXIDIZED PRODUCT OF UDMH WITH GC-MS

CHAPTER 4 NEAR INFRARED ANALYTICAL TECHNOLOGY

4.1 GENERALIZATION

4.2 BASIC PRINCIPLE OF NIR ANALYSIS

4.3 DETERMINATION OF THE COMPONENT CONTENT OF NITRIC ACID-27S

4.4. DETERMINE THE COMPONENT CONTENT OF DT-3 WITH NIR METHOD

CHAPTER 5 AUTOMATIC COUNTER OF PARTICULATE

5.1 GENERALIZATION

5.2 PRINCIPLE OF AUTOMATIC COUNTER OF PARTICULATE

5.3 DETERMINATION OF PARTICULATE CONTENT IN UDMH WITH AUTOMATIC COUNTER

PART Ⅱ ASSAY OF UDMH

CHAPTER 6 INTRODUCTION TO PROPELLANTS

6.1 CLASSIFICATION OF PROPELLANTS

6.2 FUNCTION AND CLASSIFICATION OF LIQUID PROPELLANTS

6.3 THE REQUIREMENTS FOR LIQUID PROPELLANTS

CHAPTER 7 UDMH'S USE AND MANAGEMENT

7.1 PHYSICO-CHEMICAL PROPERTIES OF UDMH

7.2 PRODUCTION AND TECHNICAL SPECIFICATION OF UDMH

7.3 TOXICITY AND ITS PROTECTION

7.4 THE DANGER OF FIRING AND EXPLOSION

7.5 MATERIAL COMPATIBILITY

7.6 STORAGE,TRANSPORTATION AND TRANFERRING

7.7 SAMPLING PRINCIPLE FOR UDMH

7.8 ATTENTIONS FOR SAFETY

CHAPTER 8 FUNDAMENTALS OF UDMH ASSAY

8.1 ACID-BASE TITRATION

8.2 MASS ANALYSIS

CHAPTER 9 ASSAY OF UDMH

9.1 TECHNICAL REQUIREMENT AND APPEARANCE INSPECTION

9.2 THE CONTENT OF UDMH,DIMETHYL AMMONIUM AND UNSYMMETRICAL HYDRAZONE DETERMINATION WITH ACID-BASE TITRATION

9.3 WATER CONTENT DETERMINATION WITH RAPID GAS MEASUREMENT

9.4 DETERMINE THE CONTENT OF UDMH,DIMETHYL AMMONIUM AND UNSYMMETRICAL HYDRAZONE WITH GAS CHROMATOGRAPHY

9.5 DETERMINATION OF THE MECHANICAL IMPURITY CONTENT IN UDMH

9.6 DETERMINATION OF DENSITY

APPENDIX 9.1 VERIFICATION OF VOLUMETERIC APPARATUS

APPENDIX 9.2 COMPOUNDING AND DETERMINATION OF STANDARD SOLUTION IN THE ASSAY OF UDMH

PART Ⅲ ASSAY OF NITRIC ACID-27S

CHAPTER 10 USE AND MANAGEMENT OF NITRIC ACID-27S

10.1 PHYSIC-CHEMICAL PROPERTIES OF NITRIC ACID-27S

10.2 USE AND MANAGEMENT OF NITRIC ACID-27S

CHAPTER 11 FUNDAMENTALS FOR THE ASSAY OF NITRIC ACID-27S

11.1 OXIDATION-REDUCTION TITRATION

11.2 GRAVIMETRY

CHAPTER 12 ASSAY OF NITRIC ACID-27S

12.1 TECHNICAL REQUIREMENTS AND APPEARANCE INSPECTION

12.2 DENSITY DETERMINATION

12.3 NITROGEN TETRAOXIDE CONTENT DETERMINATION

12.4 DETERMINATION OF WATER CONTENT

12.5 DETERMINATION OF PHOSPHORIC ACID CONTENT

12.6 DETERMINATION OF HYDROFLUORIC ACID CONTENT

12.7 DETERMINATION OF THE CONTENT OF BURNED RESIDUE

APPENDIX 12.1 THE COMPUNDING OF c(1/5 KMnO4)=0.2mol/L STANDARD SOLUTION

APPENDIX 12.2 COMPOUNDING AND DETERMINATION OF STANDARD SOLUTION IN NITRIC ACID-27S ASSAY

APPENDIX 12.3 COMPOUNDING OF INDICATORS FOR THE ASSAY OF NITRIC ACID-27S

APPENDIX 12.4 THE ERROR MATTER IN THE ASSAY OF LIQUID PROPELLANT

PART Ⅳ ASSAY OF DT-3

CHAPTER 13 ASSAY OF DT-3

13.1 COMPOUNDING OF STANDARD SOLUTIONS AND MIXED INDICATORS

13.2 SAMPLING

13.3 APPEARANCE INSPECTION

13.4 COMPONENTS ANALYSIS

13.5 WATER CONTENT ANALYSIS

13.6 PARTICLE MATTER DETERMINATION

13.7 RESIDUE DETERMINATION

APPENDIX 13.1 CALIBRATION OF PRECISION GLASS MEASURING VESSELS

APPENDIX 13.2 OPERATION OF ACIDOMETER AND NEUTRALIZITION OF FORMALDEHYDE

REFERENCE